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| Registros recuperados: 89 | |
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| Gadel, F; Charriere, B; Serve, L; Comellas, L. |
| The analysis of humic compounds by elemental analysis, PY-GC-MS and HPLC techniques permitted determination of the origin of organic inputs, essentially terrestrial, and the effects of environmental conditions in the deposits along a north-south transect through the Rhone delta, from the river mouth to the open sea. In the prodelta the sedimentation of fine particles enriches the sediments in organic matter. The humic compound contents were relatively low in sediments, perhaps due to a rapid burying of organic matter which leads to anoxic conditions. In sediments fulvic acids are more abundant than humic acids. Elemental analysis indicated that fulvic acids were enriched in hydrogen and nitrogen as compared to humic acids. Furthermore, H/C and N/C ratios... |
| Tipo: Text |
Palavras-chave: HUMIC COMPOUNDS; MOLECULAR WEIGHT CLASSES; PY-GC-MS; HPLC; RHONE DELTA. |
| Ano: 1992 |
URL: http://archimer.ifremer.fr/doc/00101/21187/18804.pdf |
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| Compiano, Am; Romano, Jc; Delagiraudiere, I; Laborde, P. |
| Samples of phytoplankton cultures and of suspended particulate matter from continental, brackish and marine waters were examined by HPLC for the monosaccharide content of their hydrolysable sugar fraction. Eight monosaccharides were currently assayed and their weight compared to HPLC-assayed chlorophyll a concentrations. With the exception of oligotrophic waters, these two variables are well correlated in the various prospected environments. Glucose was always the strongly dominant form, not only in fresh and brackish waters but also in marine samples with high phytoplanktonic biomass. If samples are compared on a salinity basis, only four monosaccharides showed significant differences in their relative concentrations, as a consequence of sampling... |
| Tipo: Text |
Palavras-chave: MONOSACCHARIDE; HPLC; PARTICULATE MATTER; SEA WATER; BRACKISH WATER. |
| Ano: 1993 |
URL: http://archimer.ifremer.fr/doc/00100/21134/18754.pdf |
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| Cariou-le Gall, Valerie; Blanchard, Gerard. |
| Chloropigments and carotenoids were measured by HPLC in an intertidal muddy sediment of Marennes-Oleron Bay (France). Concentrations were determined as a function of sediment depth at low tide. The analyses were carried out at monthly intervals over 1 yr. Pigment analysis indicated that the microphytobenthic community was dominated by diatoms throughout the sampling year. Chlorophyll b was not encountered at any time or depth, indicating that no input from macrophytic detritus had occurred at the sampling site. There was a large pool of phaeopigments a, of which phaeophorbides were the major forms (75%). A microphytobenthic bloom occurred between March and June during which phaeopigments significantly increased with a high proportion of phaeophorbides... |
| Tipo: Text |
Palavras-chave: Pigment; HPLC; Intertidal mudflat; Microphytobenthos; Seasonal change. |
| Ano: 1995 |
URL: http://archimer.ifremer.fr/doc/00257/36844/36666.pdf |
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| Brotas, V; Plantecuny, Mr. |
| A HPLC protocol is described which permits analysis of the pigment composition of coastal and intertidal sediments. The HPLC technique has been extensively applied to phytoplankton pigments for fifteen years. Papers dealing with living benthic microphytic populations have been more rare, due to complexity existing in the sediment surface, where pigments (chlorophylls and carotenoids) from several taxonomic groups of microalgae are mixed with degraded pigments from senescent phytoplankton cells and macrophytic material. The present paper describes in detail a protocol adapted from Kraay et al. (1992), which allows a good discrimination of photosynthetic pigments of microphytobenthos communities. The following procedure is recommended. Sediment samples are... |
| Tipo: Text |
Palavras-chave: Plants pigments; Sediments; Protocol; HPLC. |
| Ano: 1996 |
URL: http://archimer.ifremer.fr/doc/00096/20730/18367.pdf |
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| Mostajir, B; Bustillos-guzman, J; Claustre, H; Rassoulzadegan, F. |
| The egestion of particulate material as well as pigment degradation during microzooplankton grazing on phytoplankton are poorly known processes. In an attempt to evaluate these processes, changes in pigment concentrations within various size fractions were monitored in batch cultures of an assemblage of a pelagic ciliate (Strombidium sulcatum) and a heterotrophic flagellate (Paraphysomonas sp.) feeding on a cyanobacterium (Synechococcus sp.) over a 10-day period. Chlorophyll a, carotenoids and phaeopigments were not found in the 0.1-0.7 mu m fraction while the pigments originally in the 0.7-3.0 mu m fraction (prey) were transferred into the > 3.0 mu m size fraction (predator). During this transfer, the carotenoids (zeaxanthin and B-carotene) were not... |
| Tipo: Text |
Palavras-chave: Pigment; Phéopigment; Broutage; Protozoaire; HPLC; Pigment; Phaeopigment; Grazing; Protozoa; HPLC. |
| Ano: 1998 |
URL: http://archimer.ifremer.fr/doc/00325/43660/43209.pdf |
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| Carrão-Panizzi,Mercedes Concórdia; Beléia,Adelaide Del Pino; Kitamura,Keisuke; Oliveira,Maria Cristina Neves. |
| The effects of genetics and environmental factors on isoflavone content of soybean (Glycine max L.) cultivars grown in different locations in Brazil in 1993/94 were evaluated. Seeds of different cultivars were analised by high performance liquid chromatography (HPLC). In Rio Grande do Sul (RS), Paraná (PR), and Mato Grosso do Sul (MS) States, a significant difference in the isoflavone total content average of the cultivars IAS 5 and FT-Abyara (163.9, 116.4 and 79.5 mg/100 g, respectively) was observed. In general, IAS 5 contained higher isoflavone than FT-Abyara. Cultivars IAS 5 and FT-Abyara grown at Vacaria, RS (28°30' S latitude) with temperature average of 19°C, had the highest isoflavone concentrations (218.7 and 163.8 mg/100 g, respectively). In... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Glycine max; Daidzin; Genistin; Crop location; HPLC. |
| Ano: 1999 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-204X1999001000004 |
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| Souza,Adailson P. de; Prates,Hélio T.; Ferreira,Francisco A.; Reis,Efraim L.; Jordão,Claudio P.. |
| Em razão das poucas de informações existente na literatura, sobre a mobilidade do glyphosate e do imazapyr, em solos de baixa atividade, comum em países tropicais, foi conduzido, em laboratório, um estudo sobre a mobilidade vertical desses herbicida s em dois solos com diferente s composições químicas e fisicas. Para estudar essa mobilidade, foram utilizadas colunas de solo com diferentes alturas, as quais, após aplicação dos produtos na dose comerc ial de 4 L ha-1, foram submetida s a um regime hídrico de 40 mm h-1, por um período de 4 h. As análises dos resíduos nas diferentes profundidades foram feitas utilizando-se os métodos voltamétrico (polarografia) e HPLC, para o glyphosate e imazapyr, respectivame nte. Com base nos resultados, foi possível... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Herbicidas; Voltametria; Polarografia; Cromatografia; HPLC. |
| Ano: 1999 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-83581999000200009 |
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| Motamed, B; Texier, H. |
| Within the framework of the multi-disciplinary program Seine Aval, phenolic compounds obtained by CuO oxidation have been studied since 1995. Quantitative analyses have shown a terrestrial contribution in flood, characterized by compounds of the group P (polyols + phenol), S (syringic) and H (hydroxybenzoic). During the low water period, phenolic compounds allow a clear distinction between fluvial and estuarine suspended material. Fluvial run-off contained Syringic, Hydroxybenzoic and Vanillic phenols. In contrast, upstream penetrating marine and estuarine waters are characterized by cinnamic phenols originating from estuarine herbus. In the turbidity maximum zone, aerobic degradation of lignin material increases the (vanillic acid/vanillin) ratio. |
| Tipo: Text |
Palavras-chave: Composés phénoliques; HPLC; Matière en suspension; Seine; Phenolic compounds; HPLC; Suspended matter; Seine. |
| Ano: 2000 |
URL: http://archimer.ifremer.fr/doc/00325/43570/44051.pdf |
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| Leite,R.M.H.; Leite,R.C.; Lima,J.A.; Fóscolo,C.B.; Mota,P.M.P.C.; Lobato,F.C.F.; Lage,A.P.. |
| The high pressure liquid chromatography (HPLC) was used for the identification of isoniazid (isonicotinic acid hydrazide) in the milk of cattle treated with a dose of 25 mg/kg/day in alternated days. The effect of milk pasteurization on the isoniazid residue concentration was also studied. The drug excretion presented a cyclic variation, with higher levels in the first day after administration (aa), a mean of 1104.48µg/l, and a decrease two days aa, with a mean of 104.12µg/l. Four days after the last administration of the drug it was not possible to identify residues of isoniazid in the milk of treated animals. Body weight and milk yield influenced the amount of the excreted drug, and pasteurization decreased (mean 47.07%) the concentration of isoniazid... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Cattle; Tuberculosis; Isoniazid; Milk; HPLC. |
| Ano: 2000 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0102-09352000000600018 |
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| CASTRO,ANA HORTÊNCIA FONSÊCA; YOUNG,MARIA CLÁUDIA MARX; ALVARENGA,AMAURI ALVES DE; ALVES,JOSÉ DONIZETI. |
| In order to evaluate the influence of photoperiod on the accumulation of allantoin in comfrey (Symphytum officinale L.), a well known medicinal plant, an experiment was conducted during July and August, 1998. Cuttings obtained from 90 day old plants were submitted to four photoperiods (8, 12, 16 and 20 hours). After 60 days, allantoin content in roots and rhizomes was evaluated. The results showed that increases in photoperiod promoted an increment in the average content of allantoin in roots (0.06%, 0.303%, 1.213% and 4.78%). On the other hand, in rhizomes, allantoin accumulation decreased (9.65%, 7.14%, 0.55%) when the photoperiod was increased from 8 to 12 and 16 hours, respectively, stabilizing on a 20-hour photoperiod (0.53%). Plants cultivated under... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: HPLC; Medicinal plant; Secondary metabolism; Symphytum officinale; Ureides. |
| Ano: 2001 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-31312001000100006 |
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| OLIVEIRA,MARCELO ALVARES DE; CEREDA,MANRNEY PASCOLI; CABELLO,CLÁUDIO; URBANO,LUIZ HENRIQUE. |
| O objetivo deste trabalho foi identificar e quantificar os açúcares em frutos de pessegueiro da variedade 'Biuti', armazenados sob condições de ambiente (27,3ºC; 70% UR) e sob refrigeração (4ºC; 90%), comparar as diferenças entre os teores de açúcares nas duas condições de armazenamento. A identificação e a quantificação precisa dos açúcares (glicose, frutose e sacarose) foi realizada por cromatografia em fase líquida HPLC. Verificou-se que a sacarose foi o açúcar encontrado em maior quantidade, sendo verificado apenas traços de glicose e frutose em alguns frutos. Sob condições ambientais, os teores de sacarose do 3º até o 9º dia de armazenamento não diferiram significativamente entre si; entretanto, no 12º dia, os frutos obtiveram baixos teores de... |
| Tipo: Info:eu-repo/semantics/report |
Palavras-chave: Armazenamento; HPLC; Sacarose; Frutose e glicose. |
| Ano: 2001 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-29452001000200046 |
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| Souza,Maria Cristina Corrêa de; Benassi,Marta de Toledo; Meneghel,Renata Fraxino de Almeida; Silva,Rui Sérgio dos Santos Ferreira da. |
| The stability of orange juice obtained from a small extractor and stored in a polyethylene bottle was assessed under isothermal and non-isothermal storage conditions at 4, 8 and 12ºC for 72 hours. pH, titratable acidity and Brix did not alter significantly during the 72 hours storage. Microbiological analysis showed high initial count for moulds and yeasts that increased in the juice stored for 72h under the non-isothermal conditions with temperature abuse (12ºC/4h). Date of the sensory evaluation showed a small reduction in product acceptance in this condition. The juice, in the recommended validity period (48h), presented losses of less than 20% of the initial ascorbic acid content regardless of the treatment. However, after this time, the degradation... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Citrus fruit; Shelf life; Vitamin C; HPLC; Sensory quality; Moulds and yeasts. |
| Ano: 2004 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132004000300009 |
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| Bortoluzzi,Edson C.; Rheinheimer,Danilo dos S.; Gonçalves,Celso S.; Pellegrini,João B.R.; Zanella,Renato; Copetti,André C.C.. |
| Realizou-se este trabalho com o intuito de quantificar a presença de moléculas de agrotóxicos em águas superficiais de três unidades paisagísticas (UP) com diferentes configurações de uso, numa microbacia hidrográfica de cabeceira em Agudo, RS. Dois coletores semi-automáticos de água foram instalados no córrego de cada UP, onde se coletaram amostras, por ocasião de chuvas, em três épocas da cultura do fumo: transplante, aterramento junto aos pés da cultura (planta com 6-10 folhas) e colheita. Os princípios ativos imidacloprid, atrazina, simazina e clomazone foram quantificados por Cromatografia Líquida de Alta Eficiência com Detecção no Ultravioleta (HPLC-UV). Clorpirifós, flumetralin e iprodione foram analisados por Cromatografia Gasosa com Detecção por... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: SIG; Erosão; HPLC; Paisagem; Fumo. |
| Ano: 2006 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1415-43662006000400015 |
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| Chaves,Daniel Gonçalves; Rodrigues,Cibele Velloso; Ferreira,Wanderley Almeida; Siqueira,Pollyana Fantini Miranda; Duarte,Clara Guerra; Carneiro-Proietti,Anna Bárbara de Freitas; Santoro,Marcelo Matos. |
| In this work, polyclonal antibodies anti-human Factor IX were produced in New Zealand rabbits by immunization with commercial pure human FIX (hFIX) (Octanyne®, Octapharma, USA). The serum containing immunoglobulins anti-hFIX was useful to detect hFIX antigen in human plasma fractions submitted to anionic exchange chromatographic process and with a large yield. Immunoassays (ELISA) using bovine serum albumin, trypsin and peptides generated by cleavage assays with trypsin as digestion enzyme was performed and revealed adequate specificity of the polyclonal antibodies produced. |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Factor IX; Hemophilia B; HPLC; Purification; Antibodies; ELISA. |
| Ano: 2006 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132006000500010 |
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| Registros recuperados: 89 | |
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